Publikatsioonid, milledes on kasutatud Tartu TMR analüüsi labori seadmeid
2019:
- Tammekivi, E.; Vahur, S.; Kekišev, O.; van der Werf, I. D.; Toom, L.; Herodes, K.; Leito, I. Comparison of derivatization methods for the quantitative gas chromatographic analysis of oils. Anal. Methods 2019, Accepted Manuscript.
⇒ DOI: http://dx.doi.org/10.1039/C9AY00954J - Toom, L.; Kütt, A.; Leito, I. Simple and scalable synthesis of the carborane anion CB11H12−. Dalton Trans. 2019, 48, 7499–7502.
⇒ DOI: https://doi.org/10.1039/c9dt01062a - Parman, E.; Toom, L.; Selberg, S.; Leito, I. Determination of pKa values of fluorocompounds in water using 19F NMR. J. Phys. Org. Chem. 2019, 32, 6, e3940.
⇒ DOI: http://dx.doi.org/10.1002/poc.3940
2018:
- Vellemäe, E.; Mastitski, A.; Järv, J.; Hiltunen, J.V. A convenient methanolysis in the synthesis of carfentanyl. Org. Prep. Proced. Int. 201850, 5, 522−526.
⇒ DOI: http://dx.doi.org/10.1080/00304948.2018.1526034 - Nummert, V.; Piirsalu, M.; Toom, L.; Kesvatera, T.; Leito, I.; Koppel, I.A. Effect of charged and ortho substituents on 17O NMR chemical shifts of substituted phenyl tosylates in DMSO. J. Phys. Org.Chem. 2018, e3870.
⇒ DOI: https://doi.org/10.1002/poc.3870 - Mastitski, A.; Niinepuu, S.; Haljasorg, T.; Järv, J. One-Pot Synthesis of Protected Benzylhydrazines from Acetals. Org. Prep. Proced. Int. 201850, 4, 416-423.
⇒ DOI: https://doi.org/10.1080/00304948.2018.1468983 - Kännaste, A.; Laanisto, L.; Pazouki, L.; Copolovici, L.; Suhorutšenko, M.; Azeem, M.; Toom, L.; Borg-Karlson, A.-K.; Niinemets, Ü. Diterpenoid fingerprints in pine foliage across an environmental and chemotypic matrix: Isoabienol content is a key trait differentiating chemotypes. Phytochem 2018, 147, 80–88.
⇒ DOI: https://doi.org/10.1016/j.phytochem.2017.12.007
2017:
- Ilisson, M.; Mäeorg, U. Systematic synthesis of phthalimide-protected unsaturated hydrazine heterocycles. Synth. Commun. 2017, 47, 13, 1231–1238.
⇒ DOI: https://doi.org/10.1080/00397911.2017.1321127 - Martin, K.; Nõges, J.; Haav, K.; Kadam, S.A.; Pung, A.; Leito, I. Exploring Selectivity of 22 Acyclic Urea-, Carbazole- and Indolocarbazole-Based Receptors towards 11 Monocarboxylates. Eur. J. Org. Chem. 2017 5231–5237.
⇒ DOI: http://dx.doi.org/10.1002/ejoc.201700931 - Selberg, S.; Rodima, T.; Lõkov, M.; Tshepelevitsh, S.; Haljasorg, T.; Chhabra, S.; Kadam, S.A.; Toom, L.; Vahur, S.; Leito I. Synthesis and properties of highly lipophilic phosphazene bases. Tetrahedron Lett. 2017, 58, 2098–2102.
⇒ DOI: http://doi.org/10.1016/j.tetlet.2017.04.039 - Kestav, K.; Viht, K.; Konovalov, K.; Enkvist, E.; Uri, A.; Lavogina, D. Slowly on, Slowly off: Bisubstrate-Analogue Conjugates of 5-Iodotubercidin and Histone H3 Peptide Targeting Protein KinaseHaspin. Chembiochem 2017, 18, 790–798.
⇒ DOI: http://dx.doi.org/10.1002/cbic.201600697 - Vahter, J.; Viht, K.; Uri, A.; Enkvist, E. Oligo-aspartic acid conjugates with benzo[c][2,6]naphthyridine-8-carboxylic acid scaffold as picomolar inhibitors of CK2. Bioorg. Med. Chem. 2017, 25, 2077−2084.
⇒ DOI: http://dx.doi.org/10.1016/j.bmc.2017.02.055 - Kadam, S. A.; Haav, K.; Toom, L.; Pung, A.; Mayeux, C.; Leito, I. Multidentate anion receptors for binding glyphosate dianion: structure and affinity. Eur. J. Org. Chem. 2017, 11, 1396–1406.
⇒ DOI: http://dx.doi.org/10.1002/ejoc.201601583 - Nummert, V.; Piirsalu, M.; Vahur, S.; Toom, L.; Leito, I.; Koppel, I. A. Effects of neutral and charged substituents on the infrared carbonyl stretching frequencies in phenyl and alkyl benzoates in DMSO. J. Phys. Org. Chem. 2017, 30, e3608.
⇒ DOI: http://dx.doi.org/10.1002/poc.3608 - Tshepelevitsh, S.; Trummal, A.; Haav, K.; Martin, K.; Leito, I. Hydrogen-bond donicity in DMSO and gas phase and its dependence on Brønsted acidity. J. Phys. Chem. A 2017, 121, 357-369.
⇒ DOI: http://dx.doi.org/10.1021/acs.jpca.6b11115 - Mastitski, A.; Abramov, A.; Kruve, A.; Järv, J. Potassium iodide catalysis in the alkylation of protected hydrazines. Proc. Est. Acad. Sci. 2017, 66, 10–17.
⇒ DOI: http://dx.doi.org/10.3176/proc.2017.1.03
2016:
- Allas, Ü.; Toom, L.; Selyutina, A.; Mäeorg, U.; Medina, R.; Merits, A.; Rinken, A.; Hauryliuk, V.; Kaldalu, N.; Tenson, T. Antibacterial activity of the nitrovinylfuran G1 (Furvina) and its conversion products. Sci. Rep. 2016, 6, 36844.
⇒ DOI: http://dx.doi.org/10.1038/srep36844 - Villo, P; Matt, L.; Toom, L; Liblikas, I.; Pehk, T.; Vares, L. Hydroformylation of Olefinic Derivatives of Isosorbide and Isomannide. J. Org. Chem. 2016, 81, 7510–7517.
⇒ DOI: http://dx.doi.org/10.1021/acs.joc.6b01179 - Saame, J.; Rodima, T.; Tshepelevitsh, S.; Kütt, A.; Kaljurand, I.; Haljasorg, T.; Koppel, I.A.; Leito, I. Experimental Basicities of Superbasic Phosphonium Ylides and Phosphazenes. J. Org. Chem. 2016, 7349−7361.
⇒ DOI: http://dx.doi.org/10.1021/acs.joc.6b00872 - Kukk, S.; Järv, J. Differentiating between drugs with short and long residence times. Med. Chem. Commun. 2016, 7, 1654–1656.
⇒ DOI: http://dx.doi.org/10.1039/c6md00269b - Viira, B.; Selyutina, A.; García-Sosa, A.T.; Karonen, M.; Sinkkonen, J.; Merits, A.; Maran, U. Design, discovery, modelling, synthesis, and biological evaluation of novel and small, low toxicity s-triazine derivatives as HIV-1 non-nucleoside reverse transcriptase inhibitors. Bioorg. Med. Chem. 2016, 24, 2519-2529.
⇒ DOI: http://dx.doi.org/10.1016/j.bmc.2016.04.018
2015:
- Ilisson, M.; Tomson, K.; Selyutina, A.; Türk, S.; Mäeorg, U. Synthesis of Novel Saccharide Hydrazones. Synth. Commun. 2015, 45, 1367–1373.
⇒ DOI: http://dx.doi.org/10.1080/00397911.2015.1021425 - Kekišev, O.; Kaljurand, I.; Toom, L.; Lenoir, D.; Burk, P. Järv, J. Effect of strain on gas-phase basicity of (E)-1-methyl-2-(1-methyl-2-adamantylidene)adamantane. J. Phys. Org. Chem., 2015, 28, 447–451.
⇒ DOI: http://dx.doi.org/10.1002/poc.3435 - Kadam, S. A.; Martin, K.; Haav, K.; Toom, L.; Mayeux, C.; Pung, A.; Gale, P. A.; Hiscock, J. R.; Brooks, S. J.; Kirby, I. L.; Busschaert, N.; Leito, I. Towards the Discrimination of Carboxylates by Hydrogen-Bond Donor Anion Receptors. Chem. Eur. J., 2015, 21, 5145–5160.
⇒ DOI: http://dx.doi.org/10.1002/chem.201405858 - Mastitski, A.; Niinepuu, S.; Haljasorg, T.; Järv, J. One-pot synthesis of protected alkylhydrazines from acetals and ketals. Method scope and limitations. Organic Preparations and Procedures International 2015, 47, 490–498.
⇒ DOI: http://dx.doi.org/10.1080/00304948.2015.1088760 - Mastitski, A.; Haljasorg, T.; Kipper, K.; Järv, J. Synthesis of aza-phenylalanine, aza-tyrosine, and aza-tryptophan precursors via hydrazine alkylation. Proc. Est. Acad. Sci. 2015, 64, 168–178.
⇒ DOI: http://dx.doi.org/10.3176/proc.2015.2.05 - Kipper, A.; Kalvet, I.; Tämm, K.; Sikk, L.; Burk, P.; Kõiv, K.; Mäeorg, U. Synthesis of Unprotected CH2-Skipped Piperazine-Pyridine Alternating Cycles with Azide End-Group. Heterocycles 2015, 90, 625–630.
⇒ DOI: http://dx.doi.org/10.3987/COM-14-S(K)12 - Rebane, R.; Rodima, T.; Kütt, A.; Herodes, K. Development of amino acid derivatization reagents for liquid chromatography electrospray ionization mass spectrometric analysis and ionization efficiency measurements. J. Chromatogr. A 2015, 1390, 62–70.
⇒ DOI: http://dx.doi.org/10.1016/j.chroma.2015.02.050
2014:
- Ekambaram, R.; Enkvist, E.; Manoharan, G.; Ugandi, M.; Kasari, M.; Viht, K.; Knapp, S.; Issinger, O.-G.; Uri, A. Benzoselenadiazole-based responsive long-lifetime photoluminescent probes for protein kinases. Chem. Commun. 2014, 50, 4096–4098.
⇒ DOI: http://dx.doi.org/10.1039/C3CC49198F - Kütt, A.; Koppel, I. Pentakis(trifluoromethyl)phenol from Nitrobenzene. RSC Advances 2014, 4, 41895–41901.
⇒ DOI: http://dx.doi.org/10.1039/c4ra04540h - Teearu, A.;, Vahur, S.; Haljasorg, U.; Leito, I.; Haljasorg, T.; Toom, L. 2,5-Dihydroxybenzoic acid solution in MALDI-MS: ageing and use for mass calibration. J. Mass Spectrom. 2014, 49, 970–979.
⇒ DOI: http://dx.doi.org/10.1002/jms.3395 - Kadam, S.A.; Haav, K.; Toom, L.; Haljasorg, T.; Leito, I. NMR method for simultaneous host-guest binding constant measurement. J. Org. Chem. 2014, 79, 2501–2513.
⇒ DOI: http://dx.doi.org/10.1021/jo4027963 - Anton M.; Kisseljova, K.; Järv J. Synthesis of the Fmoc-aza-Arg(Boc)2 precursor via hydrazine alkylation. Proc. Est. Acad. Sci. 2014, 63, 438–443.
⇒ DOI: http://dx.doi.org/10.3176/proc.2014.4.09 - Mastitski, A.; Järv, J. One-Pot Synthesis of Fmoc- and Boc-Protected Aza-Methionine Precursors from 2-Methylthioacetaldehyde Dimethyl Acetal. Organic Preparations and Procedures International 2014, 46, 559–564.
⇒ DOI: http://dx.doi.org/10.1080/00304948.2014.963460
2013:
- Kütt, A.; Werner, F.; Kaljurand, I.; Leito, I.; Koppel, I. Pentakis(trifluoromethyl)benzenediazonium Cation: A Useful Building Block for the Syntheis of Trifluoromethyl-Substituted Derivatives. ChemPlusChem 2013, 78, 932–936.
⇒ DOI: http://dx.doi.org/10.1002/cplu.201300160 - Haav, K.; Kadam, S.A.; Toom, L.; Gale, P.A.; Busschaert, N.; Wenzel, M.; Hiscock, J.R.; Kirby, I.L.; Haljasorg, T.; Lőkov, M.; Leito, I. Accurate Method To Quantify Binding in Supramolecular Chemistry. J. Org. Chem. 2013, 78, 7796–7808.
⇒ DOI: http://dx.doi.org/10.1021/jo400626p